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Mobile 1200 ℃ tube furnace OTF-1200X-S-HPCVD crucible (sample stage)
Mobile 1200 ℃ tube furnace OTF-1200X-S-HPCVD crucible (sample stage)
Product details

OTF-1200X-S-HPCVD is a small open tube furnace with a crucible that can move inside the furnace tube (controlled by a stepper motor). The diameter of the furnace tube is 50mm, and the maximum operating temperature of the equipment is 1200 ℃.
Equipment features: The crucible is controlled by a stepper motor to move the furnace tube according to the set program. At the same time, a thermocouple is installed at the back of the crucible (moving with the crucible instrument), which can monitor the temperature of the sample in real time. This means that by moving the position of the crucible, the temperature required for the experiment can be accurately found in the furnace body, resulting in higher experimental accuracy and stronger repeatability. This device can be used for various experiments, such as HPCVD (hybrid physical chemical deposition), rapid thermal evaporation, and can also be used for horizontal Bridgman method to grow crystals.

Technical Parameter
High temperature furnace section

The furnace body is designed as an open type for easy replacement of furnace tubes

● Working power supply: 208-240 VAC, 50/60Hz

The maximum power is 2KW

Maximum operating temperature: 1200 ℃ (<1h)

Continuous operating temperature: 1100 ℃

Heating zone length: 200mm

Length of constant temperature zone: 60mm (+/-1 ℃ @ 1000 ℃)Note: Due to the influence of measurement methods and external environment, the measurement results may have deviations. This parameter is for reference only and should not be used as a technical indicator of the equipment. You need accurate constant temperature zone data to purchase the product. Please contact our sales personnel

● Furnace tube: high-purity quartz tube, size 50mm O.D x 44mm I.D x 450mm L)(Click on the image to view detailed information)

Temperature controller

● Adopting PID 30 segment programmed temperature control, with a temperature control accuracy of+/-1 ℃

● Temperature control instrument operation video

● Equipped with overheating and disconnection protection

The thermocouple adopts K-type thermocouple

Vacuum sealing

Using KF structure sealing flange and silicone sealing ring for sealing

There is a mechanical pressure gauge installed on the flange

The right flange is connected to a vacuum stainless steel corrugated pipe (the maximum expansion and contraction range of the stainless steel corrugated pipe is 150mm)

Vacuum degree: 10-2Torr (using mechanical pump) 10-5Torr (using molecular pump)

Crucible moving mechanism&PLC control

A 1/4 "diameter Omega armored thermocouple (K-type) is inserted into the furnace tube through a flange and can move with the crucible to monitor the actual temperature of the sample in real time

● Use a stepper motor to move the crucible (sample stage) inside the furnace tube, with a maximum stroke of 100mm and a movement accuracy of 1mm

● Set a certain distance and target position for the crucible through the touch screen, with a crucible movement speed of 180mm/min (more accurate movement speed can be customized by contacting our company, additional charges apply)

You can observe the following diagram to understand the installation method of crucible and thermocouple

Maximum heating rate and cooling rate The maximum heating rate can be obtained by moving the sample into the preheated furnace body, or by quickly removing the sample from the high-temperature furnace body to obtain the maximum cooling rate
Maximum heating rate
10℃/sec (150℃ - 250℃);
7℃/sec (250℃ - 350℃);
4℃/sec (350℃ - 500℃);
3℃/sec (500℃ - 550℃);
2℃/sec (550℃ - 650℃);
1℃/sec (650℃ - 800℃);
0.5℃/sec (800℃ - 1000℃);
Maximum cooling rate
10℃/sec (950℃ - 900℃);
7℃/sec (900℃ - 850℃);
4℃/sec (850℃ - 750℃);
2℃/sec (750℃ - 600℃);
1.5℃/sec (600℃ - 500℃);
1℃/sec (500℃ - 400℃);
0.5℃/sec (400℃ - 300℃);
Options

● Optional manual baffle valve (Figure 1)

Anti corrosion digital vacuum gauge (Figure 4)

● Quickly connect the flange for easy placement of samples (Figure 2)

A mixed gas system controlled by multiple mass flow meters, used for CVD and DVD experiments (Figure 5)

size
warranty One year warranty period, lifetime maintenance (excluding heating elements, furnace tubes, and sealing rings)
Certificate ● CE certification
All electrical components (>24V) are certified by UL/MET/CSA
If the customer incurs certification fees, our company guarantees that a single device will pass the German TUV certification or CAS certification
Precautions for use:

The pressure inside the furnace tube cannot exceed 0.02MPa

Due to the high internal pressure of the gas cylinder, a pressure reducing valve must be installed on the cylinder when introducing gas into the furnace tube. It is recommended to purchase a pressure reducing valve from our company, which has a range of 0.01MPa-0.1MPa and can be used more accurately and safely

When the temperature of the furnace body is higher than 1000 ℃, the furnace tube cannot be in a vacuum state. The pressure inside the furnace tube should be equivalent to atmospheric pressure and maintained at atmospheric pressure

The gas flow rate entering the furnace tube should be less than 200SCCM to avoid the impact of cold large airflow on the heated quartz tube

The long-term use temperature of quartz tube is less than 1100 ℃

For the experiment of sample heating, it is not recommended to close the exhaust valve and inlet valve at the flange end of the furnace tube. If it is necessary to close the gas valve to heat the sample, it is necessary to constantly pay attention to the reading on the pressure gauge. If the pressure reading is greater than 0.02 MPa, the vent valve must be opened immediately to prevent accidents (such as furnace tube rupture, flange flying out, etc.)

application

This device can be used for various experiments, and several experimental methods are listed below

RTE (rapid thermal evaporation): The evaporated material is placed in a crucible, placed in the center of the furnace, the substrate is placed on the sample stage, the sample stage is connected to the thermocouple, and then the sample stage is moved to the ideal position (where the temperature is the temperature required for the experiment)

HPCVD (Hybrid Physical Chemical Deposition): Similar to RTE, but requires a mixed gas system to mix the reaction gases and control the flow rate, while also setting the position of the evaporation material (determining the evaporation temperature of the evaporation material)

Horizontal Bridgman method for crystal growth: Place the sample and seed crystal into a crucible, and place the crucible at the center of the furnace. Then, set the crucible movement speed and slowly move the crucible

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Successful operation!

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